全文总字数：5499字
1. 毕业设计（论文）的内容和要求
本论文旨在开发一种RF/SiO2杂化气凝胶粉体的制备方法，并探索其作为原料制备碳化硅或氮化硅气凝胶的可能。
采用一步溶胶-凝胶法制备RF/SiO2杂化凝胶，经破碎制备浆料，浆料经喷雾干燥得到RF/SiO2杂化气凝胶粉体。
该课题需要突破RF/SiO2杂化凝胶浆料喷雾干燥的关键技术，制备出具有良好分散性和颗粒均匀的RF/SiO2杂化气凝胶粉体。
2. 实验内容和要求
根据毕业要求指标点3.3和4.2的要求，本课题要开展的实验内容和要求如下：（1）学习并掌握基本实验仪器(分析天平、烘箱、搅拌器、恒温水槽、喷雾干燥等)的操作方法。
（2）掌握气凝胶结构性能测试技术：熟悉利用FTIR、TG-DTA、XPS、SEM、氮气吸附等方法和设备对样品进行结构和性能测试。
（3）考察浆料的固含量、溶剂组成、研磨工艺等对RF/SiO2杂化气凝胶粉体孔结构、微观形貌、粒度的影响。
3. 参考文献
根据毕业要求指点2.3，针对复杂工程问题，具有调查研究、检索与阅读中外文献资料的能力，并能在此基础上进行归纳总结和分析论证，提出解决方案。毕业论文期间要进行研究现状调查与总结，要求在开题报告及毕业论文中查阅的中英文文献不少于30篇，其中近5年不少于10篇，英文文献不少于15篇。以下是与本课题相关的部分文献列表：1) Yong Kong*, Jiayue Zhang, Zhiyang Zhao, Xing Jiang. Monolithic silicon nitride-based aerogels with large specific surface area and low thermal conductivity. Ceramics International, 2019, 45:16331-163372) 孔勇，沈晓冬，崔升.气凝胶纳米材料.中国材料进展，2016，35（8）：1-83) Yong Kong, Xiaodong Shen, Sheng Cui, Maohong Fan. Facile synthesis of amine hybrid aerogel with high adsorption efficiency and regenerability for air capture via solvothermal-assisted sol-gel process and supercritical drying. Green Chemistry, 2015, 17: 3436-3445. 4) Yong Kong, Xiaodong Shen, Sheng Cui, Maohong Fan. Development of monolithic adsorbent via polymeric sol-gel process for low-concentration CO2 capture. Applied Energy, 2015, 147: 308-317.5) Yong Kong, Ya Zhong, Xiaodong Shen, Sheng Cui, Maohong Fan. Effect of silica sources on nanostructures of resorcinolformaldehyde/silica and carbon/silicon carbide composite aerogels. Microporous and Mesoporous Materials, 2014, 197: 77-82 6) Yong Kong, Xiaodong Shen, Sheng Cui, et al. Use of monolithic silicon carbide aerogel as a reusable support for development of regenerable CO2 adsorbent. RSC Advances, 2014, 4(109):64193-64199. 7) Yong Kong, Xiaodong Shen, Sheng Cui, et al. Preparation of monolith SiC aerogel with high surface area and large pore volume and the structural evolution during the preparation. Ceramics International, 2014, 40:8265-8271.8) Yong Kong, Xiaodong Shen, Sheng Cui, et al. Effect of carbothermal reduction temperature on microstructure of fiber reinforced silicon carbide porous monoliths with high thermal resistance. Chinese Journal of Inorganic Chemistry, 2014, 30(12):2825-2831. 9) Yong Kong, Ya Zhong, Xiaodong Shen, et al. Synthesis of monolithic mesoporous silicon carbide from resorcinol-formadehyde/silica composites. Materials Letters, 2013, 99:108-110.10) Yong Kong, Ya Zhong, Xiaodong Shen, et al. Preparation of fiber reinforced porous silicon carbide monoliths. Materials Letters, 2013, 110:141-143. 11) Yong Kong, Ya Zhong, Xiaodong Shen, et al. Synthesis and characterization of monolithic carbon/silicon carbide composite aerogels. Journal of Porous Materials, 2013, 20(4):845-849. 12) Yong Kong, Ya Zhong, Xiaodong Shen, et al. Facile synthesis of resorcinol-formaldehyde/silica composite aerogels and their transformation to monolithic carbon/silica and carbon/silicon carbide composite aerogels. Journal of Non-Crystalline Solids, 2012, 358(23):3150-3155.13) Yong Kong，Xiaodong Shen，Sheng Cui，et al. Preparation of Mesoporous α-SiC from RF/SiO2 composite aerogels. Chinese Journal of Inorganic Chemistry, 2012, 28(10): 2071-2076. 14) 孔勇，仲亚，沈晓冬，胡丹丹，崔升，滕凯明，张君君.块状低密度C/SiO2复合气凝胶的制备.南京工业大学学报（自然科学版），2012，34（4）：6-1015) K. Chen, Z. Bao, A. Du, X. Zhu, G. Wu, J. Shen, B. Zhou, Synthesis of resorcinolformaldehyde/silica composite aerogels and their low-temperature conversion to mesoporous silicon carbide, Micropor. Mesopor. Mater. 149 (2012) 1624.16) Chen X H, Yang S X, Song H H. Preparation and Characterization of RF/SiO2 Hybrid Aerogel by Sol-Gel Method [J]. Advanced Materials Research, 2006, 11(619-622.17) Li X, Chen X, Song H. Synthesis of β-SiC nanostructures via the carbothermal reduction of resorcinolformaldehyde/SiO2 hybrid aerogels [J]. Journal of Materials Science, 2009, 44(17): 4661-4667.18) 刘广文, 喷雾干燥实用技术大全. 2001: 中国轻工业出版社.19) 赵改青, 王晓波, and 刘维民, 喷雾干燥技术在制备超微及纳米粉体中的应用及展望. 材料导报, 2006(6): p. 56-59.20) 徐兵 and 赵惠忠. 前躯体-喷雾干燥法制备氧化铝超细粉体. in 第九届全国工程陶瓷学术年会.21) 施剑林, 高建华, and 林祖纕, 共沉淀喷雾干燥法制备YSZ粉料及其对烧结密度的影响. 硅酸盐学报, 1989.22) 野德武, 固含量对喷雾干燥制备氧化硅微球粒径分布的影响. 化工管理, 2014. 000(021): p. 116-116.23) 李阳兴, et al., 喷雾干燥法制备LiCoO2超细粉. 无机材料学报, 1999(4): p. 146-149.
4. 毕业设计（论文）计划
整个毕业设计（论文）课题视为一个独立项目，在进行期间，学生要按照计划有序开展，按规定时间节点完成内容，充分考虑本课题全周期、全流程管理要素。
本课题各阶段工作内容要求如下： 2021.1.10前指导老师在系统完成选题申报，学生选题。
2021.1.10~2021.1.15指导教师完成任务书下达。
以上是毕业论文任务书，课题毕业论文、开题报告、外文翻译、程序设计、图纸设计等资料可联系客服协助查找。
