全文总字数：2373字
1. 毕业设计（论文）的内容和要求
1.熟练二硫烯基离子化合物的合成2.熟练各种长晶体方法3.熟悉基本的表征手段，如PXRD、TG、IR、SCXRD4.掌握处理数据的软件，如origin、olex2
2. 实验内容和要求
1、掌握溶剂扩散法和溶剂挥发法等长单晶方法；2、掌握旋蒸仪、磁力搅拌器、烘箱等实验仪器的使用；3、熟悉X-射线单晶衍射测试、红外光谱分析、元素分析、粉末X射线衍射、热重分析、宽频介电阻抗、磁化率测试等分析方法；4、掌握实验数据处理软件的使用方法。
3. 参考文献
1. Zhu, H.; MacFarlane, D. R.; Pringle, J. M.; Forsyth, M. Organic Ionic Plastic Crystals as Solid-State Electrolytes. Trends in Chemistry 2019, 1, 126140.2. Timmermans, J. Plastic Crystals: A Historical Review. J. Phys. Chem. Solids. 1961, 18, 18.3. Alarco, P. J.; Abu-Lebdeh, Y.; Abouimrane, A.; Armand, M. The Plastic-Crystalline Phase of Succinonitrile as a Universal Matrix for Solid-State Ionic Conductors. Nat. Mater. 2004, 3, 476481.4. MacFarlane, D. R.; Forsyth, M. Plastic Crystal Electrolyte Materials: New Perspectives on Solid State Ionics. Adv. Mater. 2001, 13, 957966.5. Chang, T. H.; Hu, C. W.; Vittal, R.; Ho, K. C. Incorporation of Plastic Crystal and Transparent UV-Cured Polymeric Electrolyte in a Complementary Electrochromic Device. Solar Energy Mater. Solar Cells 2014, 126, 213218.6. Li, B.; Kawakita, Y.; Ohira-Kawamura, S.; Sugahara, T.; Wang, H.; Wang, J.; Chen, Y.; Kawaguchi, S. I.; Kawaguchi, S.; Ohara, K.; Li, K.; Yu, D.; Mole, R.;Hattori, T.; Kikuchi, T.; Yano, S.-i.; Zhang, Z.; Zhang, Z.; Ren, W.; Lin, S.; Sakata, O.; Nakajima, K.; Zhang, Z. D. Colossal Barocaloric Effects in Plastic Crystals. Nature 2019, 567, 506510.7. Lloveras, P.; Aznar, A.; Barrio, M.; Negrier, P.; Popescu, C.; Planes, A.; Maosa, L.; Stern-Taulats, E.; Avramenko, A.; Mathur, N. D.; Moya, X.; Tamarit, J.-LI. Colossal Barocaloric Effects Near Room Temperature in Plastic Crystals of Neopentylglycol. Nat. Commun. 2019, 10, 1803.8. Jin, L.; Nairn, K. M.; Forsyth, C. M.; Seeber, A. J.; MacFarlane, D. R.; Howlett, P. C.; Forsyth, M.; Pringle, J. M. Structure and Transport Properties of a Plastic Crystal Ion Conductor: Diethyl(methyl)(isobutyl)phosphonium Hexafluoro- phosphate. J. Am. Chem. Soc. 2012, 134, 96889697.9. Macfarlane, D. R.; Meakin, P.; Amini, N.; Forsyth, M. Structural Studies of Ambient Temperature Plastic Crystal Ion Conductors. J. Phys.: Condens. Matter. 2001, 13, 82578267.
4. 毕业设计（论文）计划
2020.11-2020.12 调研文献，熟悉操作过程，整理实验思路，拟定实验方案2021.1-2021.2 完成开题报告及外文翻译工作2021.3-2021.4 开展并完善实验过程，对合成产物进行表征2021.4-2021.5 对实验数据处理并分析，撰写毕业论文并修改，完成毕业答辩ppt
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