1. 毕业设计(论文)的内容和要求
毕业论文是对大学四年学习情况以及对所做的课题情况的真实反映,其内容应该包括一下方面:
1. 查阅、搜集与本课题相关的书籍和文献资料,熟悉、了解无铅铁电反铁电相变陶瓷材料的应用状况和常见的离子掺杂原理、方法。
2. 掌握传统固相法法合成BNT-BT-KNN无铅反铁电陶瓷材料的制备工艺,并分析讨论掺杂其他离子对合成BNT-BT-KNN无铅反铁电陶瓷材料的物相、形貌及尺寸的影响,并测试其铁电性能。最后,在这些基础上要总结实验操作经验及注意事项,并按要求完成毕业论文的全部内容。
2. 参考文献
[1] | 刘丽娟,杜慧玲,张晰,等. NBT-KBT-xLN系陶瓷的介电与铁电性能研究[J].人工晶体学, 2010, 39(3): 708-713. | |
[2] | 周如东,刘甜甜,刘萌萌,段 星. Sr掺杂BNT-BT压电陶瓷结构与性能研究[J]. 江苏陶瓷, 2009, 42(2): 51~55. | |
[3] | 廖梅松,陈 文,徐 庆,等. Na0.5Bi0.5TiO3-BaTiO3系无铅压电陶瓷的弛豫相变特征和铁电性能[J]. 硅酸盐学报, 2005, 33(1): 124~128. | |
[4] | 陈 文,李月明,周 静,等. (1-3x)NBT-2xKBT-xBT系无铅压电陶瓷性能研究[J]. 电子元件与材料, 2004, 11(23): 116~120. | |
[5] | 李明月, 陈 文,徐 庆,等. 四方相区NBT-KBT无铅铁电介电弛豫与铁电相变研究[J]. 人工晶体学报, 2006, 35(4): 417-421. | |
[6] | 李明月, 陈 文,徐 庆,等. Na0.5Bi0.5TiO3基无铅陶瓷的铁电相变和弛豫特性研究进展[J]. 硅酸盐学报. 2005, 33(12): 56~60. | |
[7] | 倪海民,罗来慧,诸跃进,张约品,等. Bi0.5Na0.5TiO3-BaTiO3-KNbO3陶瓷的介电特性及相变行为研究[J]. 宁波大学学报(理工版), 2011, 24(3): 473-476. | |
[8] | 王春立. 反铁电材料的应用研究[J]. 压电与声光, 1994, 16(2): 404-406 | |
[9] | 陈建华,屈绍波,高坤华,裴志斌,朱林户. 锰掺杂对(Na0.5Bi0.5)TiO3-BaTiO3-(K0.5Bi0.5)TiO3陶瓷介电和压电性能的影响[J]. 稀有金属材料与工程, 2006, 35(11): 793-796. | |
[10] | Ky-Nam Pham, Ali Hussain. Giant strain in Nb-doped Bi0.5(Na0.82K0.18)0.5TiO3 lead-free electromechanical ceramics [J]. Materials Letters 64 (2010) 22192222 | |
[11] | Ruzhong Zuo,, Chun Ye, Xusheng Fang, Jinwang Li. Tantalum doped 0.94Bi0.5Na0.5TiO30.06BaTiO3 piezoelectric ceramics [J]. Journal of the European Ceramic Society 28 (2008) 871877 | |
[12] | 贺连星,李 毅, 李广成, 李承恩. 无铅压电陶瓷材料研究进展[J].电子元件与材料, 2004,11(23):4622-4626. | |
[13] | 杨群保,荆学珍,李永祥,王 东,王天宝. 无铅压电陶瓷研究的新进展[J]. 电子元件与材料,2004, 11(23): 2622-2624. | |
[14] | Feng Gao, Xianlin Dong, Chaoliang Mao, Wei Liu, Hongling Zhang, Lihui Yang, Fei Cao, and Genshui Wang. Energy-Storage Properties of 0.89Bi0.5Na0.5TiO30.06BaTiO30.05K0.5Na0.5NbO3 Lead-Free Anti-ferroelectric Ceramics [J]. J. Am. Ceram. Soc., 2011, 94[12]: 43824386. | |
[15] | Xiaoli Tan, Cheng Ma,Joshua Frederick,Sarah Beckman, and Kyle G. Webber. The Antiferroelectric -- Ferroelectric Phase Transition in Lead‐Containing and Lead‐Free Perovskite Ceramics [J]. J Am Ceram Soc, 2011, 94(12): 43-47. | |
[18] | Jiaming Li, Feifei Wang, Xiaomei Qin, Min Xu, Wangzhou Shi. Large electrostrictive strain in lead-free Bi0.5Na0.5TiO3BaTiO3KNbO3 ceramics [J]. Appl Phys A,2011,104:72-76. | |
[19] | Shan-Tao Zhang, w Lei Wang, Yan-Feng Chen. Phase Characteristics and Piezoelectric Properties in the Bi0.5Na0.5TiO3BaTiO3K0.5Na0.5NbO3 System [J]. J. Am. Ceram. Soc., 2010,93(6):1561-1564. | |
[20] | L. A. Schmitt, J. Kling, M. Hinterstein,M. Hoelzel, Wook Jo, H.-J. Kleebe, H. Fuess. Structural investigations on lead-free Bi0.5 Na0.5 TiO3-based piezoceramics [J]. J Mater Sci ,2011,46:43684376. | |
[21] | John E. Daniels, Wook Jo, Jurgen Rodel, Veijo Honkimaki, Jacob L. Jones. Electric-field-induced phase-change behavior in (Bi0.5Na0.5)TiO3-BaTiO3-K0.5Na0.5NbO3 [J]. Acta Materialia 58 (2010) 21032111. | |
[22] | YUE-MING LI, WEN CHEN,QING XU,JING ZHOU,1HUA-JUN SUN , MEI-SONG LIAO. Dielectric and piezoelectric properties of Na0.5Bi 0.5TiO3-K0.5Bi0.5TiO 3-NaNbO3lead-free ceramics [J]. Journal of Electroceramics, 14, 5358, 2005 | |
[23] | Xiu-Cheng Zheng, Guang-Ping Zheng, Zheng Lin, Zhi-Yuan Jiang. Electro-caloric behaviors of lead-free Bi0.5Na0.5TiO3-BaTiO3 ceramics [J]. J Electroceram (2012) 28:2026. |
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