基于Zr-MOFs类质子导体及其复合膜的制备和质子导电研究任务书

 2022-02-10 18:34:30

全文总字数：2686字

1. 毕业设计（论文）的内容和要求

1.熟练掌握Zr-MOFs类化合物合成方法2.掌握复合膜制备方法3.掌握基本表征和检测方法，如PXRD、电化学工作站等4.熟悉数据处理以及画图软件，如origin等5.自主撰写和修改毕业论文

2. 实验内容和要求

1. 通过溶剂热法制备Zr-MOFs；2. 掌握烘箱、旋转蒸发仪，油浴锅等实验仪器的使用方法；3. 熟悉电化学工作站，X粉末射线衍射等各种表征仪器的使用；4. 掌握实验数据处理软件使用方法；5. 掌握对实验数据理解与分析能力。

3. 参考文献

1. Luo, H. B.; Ren, Q.; Wang, P.; Zhang, J.; Wang, L. F.; Ren, X. M. High Proton Conductivity Achieved by Encapsulation of Imidazole Molecules into Proton-Conducting MOF-808. ACS Appl. Mater. Interfaces 2019, 11 (9), 9164-9171.2. Luo, H. B.; Wang, M.; Zhang, J.; Tian, Z. F.; Zou, Y.; Ren, X. M. Open-Framework Chalcogenide Showing Both Intrinsic Anhydrous and Water-Assisted High Proton Conductivity. ACS Appl. Mater. Interfaces 2018, 10, 2619-2627.3.Xing, W. H.; Li, H. Y.; Dong, X. Y.; Zang, S. Q. Robust Multifunctional Zr-based Metal-Organic Polyhedra for High Proton Conductivity and Selective CO2 Capture. J. Mater. Chem. A 2018, 6, 7724-7730.4. Li, A. L.; Gao, Q.; Xu, J.; Bu, X. H. Proton-Conductive Metal-Organic Frameworks: Recent Advances and Perspectives. Coord. Chem. Rev. 2017, 344, 54-82.5. Wu, L.; Yang, Y.; Ye, Y.; Yu, Z.; Song, Z.; Chen, S.; Chen, L.; Zhang, Z.; Xiang, S. Loading Acid-Base Pairs into Periodic Mesoporous Organosilica for High Anhydrous Proton Conductivity over a Wide Operating Temperature Window. ACS Appl. Energy Mater. 2018, 1, 5068-5074.6. Peng, Y.; Huang, H.; Zhang, Y.; Kang, C.; Chen, S.; Song, L.; Liu, D.; Zhong, C. A versatile MOF-based Trap for Heavy Metal Ion Capture and Dispersion. Nat. Commun. 2018, 9, 187.7. Yan, X.; Wang, K.; Xu, X.; Wang, S.; Ning, Q.; Xiao, W.; Zhang, N.; Chen, Z.; Chen, C. Bronsted Basicity in Metal-Organic Framework-808 and Its Application in Base-Free Catalysis. Inorg. Chem. 2018, 57, 8033-8036.8. Sadakiyo, M.; Yamada, T.; Kitagawa, H. Rational Designs for Highly Proton-Conductive Metal-Organic Frameworks. J. Am. Chem. Soc. 2009, 131, 9906-9907.9. Wang, J. X.; Wang, Y. D.; Wei, M. J.; Tan, H. Q.; Wang, Y. H.; Zang, H. Y.; Li, Y. G. Inorganic Open Framework based on Lanthanide Ions and Polyoxometalates with High Proton Conductivity. Inorg. Chem. Front. 2018, 5, 1213-1217.10. Xing, W. H.; Li, H. Y.; Dong, X. Y.; Zang, S. Q. Robust Multifunctional Zr-based Metal-Organic Polyhedra for High Proton Conductivity and Selective CO2 Capture. J. Mater. Chem. A 2018, 6, 7724-7730.11. Campbell, M. G.; Liu, S. F.; Swager, T. M.; Dinc, M. Chemiresistive Sensor Arrays from Conductive 2D MetalOrganic Frameworks. J. Am. Chem. Soc. 2015, 137, 13780-13783.

4. 毕业设计（论文）计划

2020.11-2020-12调研文献，设计实验方案和检测项目2021.1-2021.2 完成开题报告与外文文献翻译工作2021.3-2020.4 开展实验项目，对合成产物进行表征2021.4-2021.5 对实验数据分析处理，完成毕业论文和毕业答辩PPT

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